By G. Schudt-Weitz, I. Strell (auth.), K.-H. Hellwege, A. M. Hellwege (eds.)
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045. Ruby-red, thin plates. *Or Pba2. Colourless plates elongated along b; other canonical forms are given. Film data; anisotropic refinement. 189”C. 099. 17 H20 \O -2 HN-N’ / N-NH 3174 ‘N-NH No. -No. C,6H2404 Brefcldin A; [lS-(1 R*,2E,6R*,10E,1laR*,13R*,14aS*)]-1,6,7,8,9. 1la,12,13,14,14a-Decahydro-1,13-dihydroxy-6-methyl-4H-cyclopentV]oxacyclotridecin-4-one P2,&2, 14 3 I ;$, Formula wt. Additional remarks. Further informations. R. Footnotes. 21 y&)0) Colourless prismatic needles (from methanol/acetone).
071. See also LB 17-12-8. Needles (from toluene). Colour Index Pigment Red 3. *Or P2,/m. y;ji:, ... 1.. 4) ... Soluble in NJ-dimethylformamide. y3’ Soluble in NJ-dimethylformamide. Diffractometer measurement; anisotropic refinement; hydrogen positions determined. 026. 6) Red crystals; diamagnetic; soluble in acetone; insoluble in ether. light petroleum. Film data. -195”C (decomposed). 13. f7ar~us Link ex Fries. Film data; diffractometer measurement; anisotropic retincment; hydrogen positions determined.
1 Formula wt. 423 Additional remarks. Further informations. R. Footnotes. 362R , S,- S,: 2,304A. Film data; anisotropic retincment ; hydrogen positions dctcrmined. 071. See also LB 17-12-8. Needles (from toluene). Colour Index Pigment Red 3. *Or P2,/m. y;ji:, ... 1.. 4) ... Soluble in NJ-dimethylformamide. y3’ Soluble in NJ-dimethylformamide. Diffractometer measurement; anisotropic refinement; hydrogen positions determined. 026. 6) Red crystals; diamagnetic; soluble in acetone; insoluble in ether.